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Abstract
Pyrene-2-carboxylic acid is a versatile intermediate for introducing the unusual 2-pyrenyl unit into functional organic molecules. A classical preparation for this molecule has been revised and improved to give a robust and efficient three-step process. The method has been applied on a multigram scale to give pyrene-2-carboxylic acid in >70% overall yield from pyrene.
Original language | English |
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Article number | st-2014-d0576-l |
Pages (from-to) | 2591-2594 |
Number of pages | 4 |
Journal | SYNLETT |
Volume | 25 |
Issue number | 18 |
DOIs | |
Publication status | Published - Nov 2014 |
Keywords
- condensed aromatic compounds
- electrophilic aromatic substitution
- ring closure
- ring opening
- Haller-Bauer cleavage
- 2,7-FUNCTIONALIZED PYRENE DERIVATIVES
- POLYCYCLIC AROMATIC-HYDROCARBONS
- CARBON NANOTUBES
- DNA MODIFICATION
- NUCLEIC-ACIDS
- HALLER-BAUER
- PI-STACKING
- CLEAVAGE
- PROBES
- BORYLATION
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From "temples" to "courtyards" for carbohydrate recognition - expanding the scope of synthetic lectins.
1/10/11 → 1/10/14
Project: Research