Accelerating quantitative 13C NMR spectra using an EXtended ACquisition Time (EXACT) method

Zahra H. Al-Aasmi; Alexandra Shchukina; Craig P. Butts

doi:10.1039/d2cc01768g

Accelerating quantitative ¹³C NMR spectra using an EXtended ACquisition Time (EXACT) method

Zahra H. Al-Aasmi, Alexandra Shchukina, Craig P. Butts^*

^*Corresponding author for this work

Research output: Contribution to journal › Article (Academic Journal) › peer-review

6 Citations (Scopus)

235 Downloads (Pure)

Abstract

Accurate quantitative ¹³C NMR spectra can be accelerated by using EXACT (EXtended ACquisition Time) NMR methods which reduce Nuclear Overhauser Enhancement (NOE) during the FID. This allows 30-50% shorter experiment times to be used when achieving a given level of quantitative accuracy.

Original language	English
Pages (from-to)	7781-7784
Number of pages	4
Journal	Chemical Communications
Volume	58
Issue number	56
Early online date	8 Jun 2022
DOIs	https://doi.org/10.1039/d2cc01768g
Publication status	E-pub ahead of print - 8 Jun 2022

Bibliographical note

Publisher Copyright:
© 2022 The Royal Society of Chemistry

Research Groups and Themes

Organic & Biological

Access to Document

10.1039/d2cc01768gLicence: CC BY

Full-text PDF (final published version)
This is the final published version of the article (version of record). It first appeared online via RSC at https://doi.org/10.1039/D2CC01768G . Please refer to any applicable terms of use of the publisher.
Final published version, 2.2 MBLicence: CC BY

Handle.net

Persistent link

Cite this

@article{7320479b882d4b41bc84b7e8d08c501b,

title = "Accelerating quantitative 13C NMR spectra using an EXtended ACquisition Time (EXACT) method",

abstract = "Accurate quantitative 13C NMR spectra can be accelerated by using EXACT (EXtended ACquisition Time) NMR methods which reduce Nuclear Overhauser Enhancement (NOE) during the FID. This allows 30-50\% shorter experiment times to be used when achieving a given level of quantitative accuracy.",

author = "Al-Aasmi, \{Zahra H.\} and Alexandra Shchukina and Butts, \{Craig P.\}",

note = "Publisher Copyright: {\textcopyright} 2022 The Royal Society of Chemistry",

year = "2022",

month = jun,

day = "8",

doi = "10.1039/d2cc01768g",

language = "English",

volume = "58",

pages = "7781--7784",

journal = "Chemical Communications",

issn = "1359-7345",

publisher = "Royal Society of Chemistry",

number = "56",

}

TY - JOUR

T1 - Accelerating quantitative 13C NMR spectra using an EXtended ACquisition Time (EXACT) method

AU - Al-Aasmi, Zahra H.

AU - Shchukina, Alexandra

AU - Butts, Craig P.

PY - 2022/6/8

Y1 - 2022/6/8

N2 - Accurate quantitative 13C NMR spectra can be accelerated by using EXACT (EXtended ACquisition Time) NMR methods which reduce Nuclear Overhauser Enhancement (NOE) during the FID. This allows 30-50% shorter experiment times to be used when achieving a given level of quantitative accuracy.

AB - Accurate quantitative 13C NMR spectra can be accelerated by using EXACT (EXtended ACquisition Time) NMR methods which reduce Nuclear Overhauser Enhancement (NOE) during the FID. This allows 30-50% shorter experiment times to be used when achieving a given level of quantitative accuracy.

UR - https://www.scopus.com/pages/publications/85132897479

U2 - 10.1039/d2cc01768g

DO - 10.1039/d2cc01768g

M3 - Article (Academic Journal)

C2 - 35731109

AN - SCOPUS:85132897479

SN - 1359-7345

VL - 58

SP - 7781

EP - 7784

JO - Chemical Communications

JF - Chemical Communications

IS - 56

ER -