Rapid and safe ASAP acquisition with EXACT NMR

I E Ndukwe; A Shchukina; K Kazimierczuk; C P Butts

doi:10.1039/c6cc07140f

Rapid and safe ASAP acquisition with EXACT NMR

I E Ndukwe, A Shchukina, K Kazimierczuk, C P Butts

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Abstract

The dangerously high power levels required for fast ASAP-HSQC and ASAP-HMQC experiments are mitigated by employing EXACT NMR. The utility of this technique is demonstrated by application of the EXACT ASAP-HSQC to chemical reaction monitoring, accelerating data acquisition by up to 2 orders of magnitude - providing evidence of it's value in fast quantitative NMR processes.

Original language	English
Pages (from-to)	12769-12772
Number of pages	4
Journal	Chemical Communications
Volume	52
Issue number	86
Early online date	6 Oct 2016
DOIs	https://doi.org/10.1039/c6cc07140f
Publication status	Published - 20 Oct 2016

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Organic & Biological

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10.1039/c6cc07140f

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This is the author accepted manuscript (AAM). The final published version (version of record) is available online via RSC at http://pubs.rsc.org/en/Content/ArticleLanding/2016/CC/C6CC07140F#!divAbstract. Please refer to any applicable terms of use of the publisher.
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A 13C NMR Coldprobe to Underpin Chemistry Research.
Butts, C. P. (Principal Investigator)
28/02/14 → 29/11/17
Project: Research

Professor Craig P Butts
- Craig.Buttsbristol.acuk
- School of Chemistry - Head of School, Professor of Structural and Mechanistic Chemistry
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Cite this

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title = "Rapid and safe ASAP acquisition with EXACT NMR",

abstract = "The dangerously high power levels required for fast ASAP-HSQC and ASAP-HMQC experiments are mitigated by employing EXACT NMR. The utility of this technique is demonstrated by application of the EXACT ASAP-HSQC to chemical reaction monitoring, accelerating data acquisition by up to 2 orders of magnitude - providing evidence of it's value in fast quantitative NMR processes.",

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AU - Shchukina, A

AU - Kazimierczuk, K

AU - Butts, C P

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AB - The dangerously high power levels required for fast ASAP-HSQC and ASAP-HMQC experiments are mitigated by employing EXACT NMR. The utility of this technique is demonstrated by application of the EXACT ASAP-HSQC to chemical reaction monitoring, accelerating data acquisition by up to 2 orders of magnitude - providing evidence of it's value in fast quantitative NMR processes.

U2 - 10.1039/c6cc07140f

DO - 10.1039/c6cc07140f

M3 - Article (Academic Journal)

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VL - 52

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EP - 12772

JO - Chemical Communications

JF - Chemical Communications

IS - 86

ER -

Rapid and safe ASAP acquisition with EXACT NMR

Abstract

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A 13C NMR Coldprobe to Underpin Chemistry Research.

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Professor Craig P Butts

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