The HXD95: A modified Bassett-type hydrothermal diamond anvil cell for in situ XRD experiments up to 5 GPa and 1300 K

Marion Louvel; James W. E. Drewitt; Allan Ross; Richard Thwaites; Benedict J. Heinen; Dean S. Keeble; Christine M. Beavers; Michael J. Walter; Simone Anzellini

doi:10.1107/S1600577519016801

The HXD95: A modified Bassett-type hydrothermal diamond anvil cell for in situ XRD experiments up to 5 GPa and 1300 K

Marion Louvel, James W. E. Drewitt, Allan Ross, Richard Thwaites, Benedict J. Heinen, Dean S. Keeble, Christine M. Beavers, Michael J. Walter, Simone Anzellini

School of Earth Sciences

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Abstract

We report a new diamond anvil cell apparatus for in situ synchrotron X-ray diffraction measurements of liquids and glasses at pressures from ambient to 5 GPa and temperatures from ambient to 1300 K. This portable set-up enables in situ monitoring of melting of complex compounds, and the determination of the structure and properties of melts under moderately high-pressure and hightemperature conditions relevant to industrial processes and magmatic processes in Earth’s crust and shallow mantle. The device was constructed according to a modified Bassett-type hydrothermal diamond-anvil cell design with a large angular opening ( = 95°). In this paper, we report the successful application of this device to record in situ synchrotron X-ray diffraction of liquid Ga and synthetic PbSiO3 glass to 1100 K and 3 GPa.

Original language	English
Pages (from-to)	529-537
Number of pages	9
Journal	Journal of Synchrotron Radiation
Volume	27
Issue number	2
DOIs	https://doi.org/10.1107/S1600577519016801
Publication status	Published - 1 Mar 2020

Keywords

diamond-anvil cells
resistive heating
synchrotron characterization
metallic liquids
glasses and melts
extreme conditions

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10.1107/S1600577519016801

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Deep Water: Hydrous Silicate Melts and the Transition Zone Water Filter
Lord, O. T. (Principal Investigator)
12/10/16 → 31/10/20
Project: Research

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title = "The HXD95: A modified Bassett-type hydrothermal diamond anvil cell for in situ XRD experiments up to 5 GPa and 1300 K",

abstract = "We report a new diamond anvil cell apparatus for in situ synchrotron X-ray diffraction measurements of liquids and glasses at pressures from ambient to 5 GPa and temperatures from ambient to 1300 K. This portable set-up enables in situ monitoring of melting of complex compounds, and the determination of the structure and properties of melts under moderately high-pressure and hightemperature conditions relevant to industrial processes and magmatic processes in Earth{\textquoteright}s crust and shallow mantle. The device was constructed according to a modified Bassett-type hydrothermal diamond-anvil cell design with a large angular opening ( = 95°). In this paper, we report the successful application of this device to record in situ synchrotron X-ray diffraction of liquid Ga and synthetic PbSiO3 glass to 1100 K and 3 GPa.",

keywords = "diamond-anvil cells, resistive heating, synchrotron characterization, metallic liquids, glasses and melts, extreme conditions",

author = "Marion Louvel and Drewitt, {James W. E.} and Allan Ross and Richard Thwaites and Heinen, {Benedict J.} and Keeble, {Dean S.} and Beavers, {Christine M.} and Walter, {Michael J.} and Simone Anzellini",

year = "2020",

month = mar,

day = "1",

doi = "10.1107/S1600577519016801",

language = "English",

volume = "27",

pages = "529--537",

journal = "Journal of Synchrotron Radiation",

issn = "0909-0495",

publisher = "International Union of Crystallography",

number = "2",

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TY - JOUR

T1 - The HXD95

T2 - A modified Bassett-type hydrothermal diamond anvil cell for in situ XRD experiments up to 5 GPa and 1300 K

AU - Louvel, Marion

AU - Drewitt, James W. E.

AU - Ross, Allan

AU - Thwaites, Richard

AU - Heinen, Benedict J.

AU - Keeble, Dean S.

AU - Beavers, Christine M.

AU - Walter, Michael J.

AU - Anzellini, Simone

PY - 2020/3/1

Y1 - 2020/3/1

N2 - We report a new diamond anvil cell apparatus for in situ synchrotron X-ray diffraction measurements of liquids and glasses at pressures from ambient to 5 GPa and temperatures from ambient to 1300 K. This portable set-up enables in situ monitoring of melting of complex compounds, and the determination of the structure and properties of melts under moderately high-pressure and hightemperature conditions relevant to industrial processes and magmatic processes in Earth’s crust and shallow mantle. The device was constructed according to a modified Bassett-type hydrothermal diamond-anvil cell design with a large angular opening ( = 95°). In this paper, we report the successful application of this device to record in situ synchrotron X-ray diffraction of liquid Ga and synthetic PbSiO3 glass to 1100 K and 3 GPa.

AB - We report a new diamond anvil cell apparatus for in situ synchrotron X-ray diffraction measurements of liquids and glasses at pressures from ambient to 5 GPa and temperatures from ambient to 1300 K. This portable set-up enables in situ monitoring of melting of complex compounds, and the determination of the structure and properties of melts under moderately high-pressure and hightemperature conditions relevant to industrial processes and magmatic processes in Earth’s crust and shallow mantle. The device was constructed according to a modified Bassett-type hydrothermal diamond-anvil cell design with a large angular opening ( = 95°). In this paper, we report the successful application of this device to record in situ synchrotron X-ray diffraction of liquid Ga and synthetic PbSiO3 glass to 1100 K and 3 GPa.

KW - diamond-anvil cells

KW - resistive heating

KW - synchrotron characterization

KW - metallic liquids

KW - glasses and melts

KW - extreme conditions

U2 - 10.1107/S1600577519016801

DO - 10.1107/S1600577519016801

M3 - Article (Academic Journal)

C2 - 32153294

SN - 0909-0495

VL - 27

SP - 529

EP - 537

JO - Journal of Synchrotron Radiation

JF - Journal of Synchrotron Radiation

IS - 2

ER -

The HXD95: A modified Bassett-type hydrothermal diamond anvil cell for in situ XRD experiments up to 5 GPa and 1300 K

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Deep Water: Hydrous Silicate Melts and the Transition Zone Water Filter

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